PL80470B1 - 2,4-dihydroxybenzophenone[FR2034934A1] - Google Patents
2,4-dihydroxybenzophenone[FR2034934A1] Download PDFInfo
- Publication number
- PL80470B1 PL80470B1 PL13938670A PL13938670A PL80470B1 PL 80470 B1 PL80470 B1 PL 80470B1 PL 13938670 A PL13938670 A PL 13938670A PL 13938670 A PL13938670 A PL 13938670A PL 80470 B1 PL80470 B1 PL 80470B1
- Authority
- PL
- Poland
- Prior art keywords
- acetic acid
- water
- dihydroxybenzophenone
- chloride
- reaction
- Prior art date
Links
- ZXDDPOHVAMWLBH-UHFFFAOYSA-N 2,4-Dihydroxybenzophenone Chemical compound OC1=CC(O)=CC=C1C(=O)C1=CC=CC=C1 ZXDDPOHVAMWLBH-UHFFFAOYSA-N 0.000 title claims description 13
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract description 39
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 claims abstract description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 238000006243 chemical reaction Methods 0.000 claims abstract description 9
- 238000000034 method Methods 0.000 claims description 13
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 9
- 238000002360 preparation method Methods 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims 2
- 239000007858 starting material Substances 0.000 abstract description 5
- 239000004033 plastic Substances 0.000 abstract description 3
- 229920003023 plastic Polymers 0.000 abstract description 3
- 239000006096 absorbing agent Substances 0.000 abstract description 2
- XEMRAKSQROQPBR-UHFFFAOYSA-N (trichloromethyl)benzene Chemical compound ClC(Cl)(Cl)C1=CC=CC=C1 XEMRAKSQROQPBR-UHFFFAOYSA-N 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 238000003786 synthesis reaction Methods 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 description 5
- 239000011541 reaction mixture Substances 0.000 description 5
- MTZQAGJQAFMTAQ-UHFFFAOYSA-N ethyl benzoate Chemical compound CCOC(=O)C1=CC=CC=C1 MTZQAGJQAFMTAQ-UHFFFAOYSA-N 0.000 description 4
- JFDZBHWFFUWGJE-UHFFFAOYSA-N benzonitrile Chemical compound N#CC1=CC=CC=C1 JFDZBHWFFUWGJE-UHFFFAOYSA-N 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 description 2
- 229910015900 BF3 Inorganic materials 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 229910021627 Tin(IV) chloride Inorganic materials 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- PASDCCFISLVPSO-UHFFFAOYSA-N benzoyl chloride Chemical compound ClC(=O)C1=CC=CC=C1 PASDCCFISLVPSO-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- WTEOIRVLGSZEPR-UHFFFAOYSA-N boron trifluoride Chemical compound FB(F)F WTEOIRVLGSZEPR-UHFFFAOYSA-N 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- FAIAAWCVCHQXDN-UHFFFAOYSA-N phosphorus trichloride Chemical compound ClP(Cl)Cl FAIAAWCVCHQXDN-UHFFFAOYSA-N 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000012429 reaction media Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
- HPGGPRDJHPYFRM-UHFFFAOYSA-J tin(iv) chloride Chemical compound Cl[Sn](Cl)(Cl)Cl HPGGPRDJHPYFRM-UHFFFAOYSA-J 0.000 description 1
- 239000006097 ultraviolet radiation absorber Substances 0.000 description 1
- 235000005074 zinc chloride Nutrition 0.000 description 1
- 239000011592 zinc chloride Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/008—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reaction with tri- or tetrahalomethyl compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| HUBO001175 | 1969-03-14 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PL80470B1 true PL80470B1 (en) | 1975-08-30 |
Family
ID=10993690
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL13938670A PL80470B1 (en) | 1969-03-14 | 1970-03-13 | 2,4-dihydroxybenzophenone[FR2034934A1] |
Country Status (10)
| Country | Link |
|---|---|
| JP (1) | JPS4829218B1 (en]) |
| BE (1) | BE747317A (en]) |
| BG (1) | BG17515A3 (en]) |
| CS (1) | CS153542B2 (en]) |
| DE (1) | DE2010535A1 (en]) |
| FR (1) | FR2034934A1 (en]) |
| NL (1) | NL7003489A (en]) |
| PL (1) | PL80470B1 (en]) |
| RO (1) | RO55296A (en]) |
| YU (1) | YU33386B (en]) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS52107434A (en) * | 1977-03-11 | 1977-09-09 | Nissan Diesel Motor Co Ltd | Exhaust purifier of internal combustion engine |
| US4568429A (en) * | 1984-03-02 | 1986-02-04 | Gaf Corporation | Process for the preparation of 2,4-dihydroxybenzophenones |
-
1970
- 1970-03-02 YU YU62670A patent/YU33386B/xx unknown
- 1970-03-05 DE DE19702010535 patent/DE2010535A1/de active Pending
- 1970-03-10 FR FR7008569A patent/FR2034934A1/fr active Granted
- 1970-03-11 NL NL7003489A patent/NL7003489A/xx unknown
- 1970-03-12 BG BG014159A patent/BG17515A3/xx unknown
- 1970-03-13 RO RO6275470A patent/RO55296A/ro unknown
- 1970-03-13 PL PL13938670A patent/PL80470B1/pl unknown
- 1970-03-13 BE BE747317A patent/BE747317A/xx unknown
- 1970-03-14 JP JP2191570A patent/JPS4829218B1/ja active Pending
- 1970-03-16 CS CS172070A patent/CS153542B2/cs unknown
Also Published As
| Publication number | Publication date |
|---|---|
| JPS4829218B1 (en]) | 1973-09-08 |
| BE747317A (fr) | 1970-08-17 |
| CS153542B2 (en]) | 1974-02-25 |
| FR2034934A1 (en) | 1970-12-18 |
| NL7003489A (en]) | 1970-09-16 |
| BG17515A3 (bg) | 1973-11-10 |
| YU33386B (en) | 1976-12-31 |
| FR2034934B1 (en]) | 1975-12-26 |
| RO55296A (en]) | 1973-05-17 |
| DE2010535A1 (de) | 1970-10-01 |
| YU62670A (en) | 1976-06-30 |
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